Bleach 121 - Clash! The Protector vs. The Bearer
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Credit for summary: Wikipedia
With their power limits lifted, Hitsugaya, Rangiku and Renji easily dispatch their opponents. Meanwhile, Ichigo is overpowered by Grimmjow, who is able to fight against Ichigo barehanded. Ichigo uses his Getsuga Tensho, which slightly damages Grimmjow and awakens his inner hollow. Before Grimmjow can release his zanpakuto, Kaname Tosen arrives. Tosen takes Grimmjow back to Hueco Mundo, claiming that he violated Aizen's orders by attacking the real world.